7342 |
11 |
Fe–N-rGO |
|
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7343 |
12 |
CeO2@ZIF-8 NPs |
275 |
|
nm |
TEM |
the average |
651.2260 |
|
|
|
|
|
|
|
7344 |
14 |
CeONPs |
10 |
|
nm |
TEM |
|
88.6 |
|
|
|
|
|
|
|
7345 |
15 |
PEG–TiO1+x |
1.8 ± 0.67 nm (width) × 28.68 ± 4.24 nm (length) |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7346 |
17 |
MoO3–x NUs |
142.8 |
13.3 |
nm |
TEM |
|
|
|
|
|
|
|
|
|
7347 |
20 |
HMON-Au@Cu-TA |
64 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7348 |
21 |
Fe-N/C |
120 |
|
nm |
SEM |
The as-synthesized Fe-Zn ZIFs exhibited a well-defined rhombic dodecahedron shape and smooth surface with diameters of 2.2 μm, 400 nm, 120 nm and 35 nm (SEM, Fig. S1), respectively. |
996.02 |
|
|
|
|
|
|
|
7349 |
23 |
Co3O4@Co-Fe oxide double-shelled nanocages (DSNCs) |
1250 |
|
nm |
SEM |
|
12.16 |
|
|
|
|
|
|
|
7351 |
24 |
core–shell UMOFs@Au NPs |
81.6 |
|
nm |
TEM |
|
284.52 |
|
|
|
|
|
|
|
7350 |
24 |
core–shell–shell UCNPs |
29.8 |
2.2 |
nm |
TEM |
|
|
|
|
|
|
|
|
|
7352 |
27 |
Cu-N-C SAzymes |
1.1 |
|
nm |
AFM |
The thickness of Cu-N-C SAzyme is about 1.1nm. |
|
|
|
|
|
|
|
|
7353 |
29 |
PDA‐Pt‐CD@RuFc NPs |
290 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7354 |
31 |
FeS2 NPs |
200 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7355 |
32 |
Au2Pt |
42 |
3 |
nm |
TEM |
|
|
|
|
|
|
|
|
|
7356 |
33 |
Co/PMCS |
|
|
|
|
|
|
|
|
|
|
|
|
|
7357 |
35 |
Cu5.4O USNPs |
3.5-4.0 |
|
nm |
TEM |
The average hydrodynamic diameter of Cu5.4O USNPs was approximately 4.5 nm. |
|
|
|
|
|
|
|
|
7358 |
38 |
Pt@PCN222-Mn |
200 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7359 |
39 |
Au@Rh‐ICG‐CM |
95.6 |
3.6 |
nm |
DLS |
The mean diameter of Au@Rh nanoparticles is 95.6 ± 3.6 nm. |
|
|
|
|
|
|
|
|
7360 |
40 |
MoS2/g-C3N4 HNs |
|
|
|
TEM and HRTEM |
the fringes are widely separated with the spacing of 0.323 nm are in agreement with the (002) plane of the g-C3N4 and the lattice spacing of 0.628 nm |
|
|
|
|
|
|
|
|
7361 |
42 |
Atv/PTP-TCeria NPs |
8.16 |
1.98 |
nm |
TEM |
the average sizes 8.16±1.98 nm |
|
|
|
|
|
|
U/mg |
|
7362 |
44 |
Sm-TCPP-Pt |
|
|
nm |
TEM |
nanoplate morphology (∼100 nm in diameter) and ultrathin thickness (<10 nm) |
|
|
|
|
|
|
|
|
7363 |
45 |
Au40/γ-CD-MOF |
∼264 |
|
nm |
Others |
γ-CD-MOF at ∼264 nm |
|
|
|
|
|
|
|
|
7364 |
47 |
CuTA |
|
|
nm |
TEM |
an average length and width of 140.5 and 36.9 nm |
|
|
|
|
|
|
|
|
7365 |
48 |
Fe-NC nanozymes |
∼1.8 |
|
nm |
AFM |
AFM measurement demonstrates that the thickness of ultrathin nanosheets is ∼1.8 nm |
|
|
|
|
25 |
|
U/mg |
|
7366 |
49 |
Lipo-OGzyme-AIE |
122.5 |
|
nm |
TEM |
the mean diameter increased from 96.8 nm of Lipo-AIE to 122.5 nm of the Lipo-OGzyme-AIE |
|
|
|
|
|
|
|
|
7367 |
52 |
EPL-coated MnO2 nanosheets (EM) |
~330.86 |
|
nm |
TEM |
the size of the MnO2 nanosheet was measured to be around 330.86 nm |
|
|
|
|
|
|
|
|
7368 |
54 |
Fe3C/N–C |
4–5 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7369 |
56 |
MOF-546(Fe) |
|
|
|
SEM |
a length of about 1–2 μm and a diameter of about 0.5–1 μm |
|
|
|
μmol/min |
6 |
-2 |
μmol glucose/(mg GOx·min) |
|
7370 |
60 |
Cu2MoS4 (CMS)/Au |
106.57 |
|
nm |
DLS |
and the polymer dispersity index is 0.228 |
|
|
|
|
|
|
|
|
7371 |
61 |
Fe3O4-TiO2/rGO (FTG) |
9 |
0.2 |
nm |
TEM |
Fe3O4 and TiO2 |
|
|
|
|
|
|
|
|
7372 |
63 |
Co-based homobimetallic hollow nanocages |
700-1000 |
|
nm |
TEM |
Co based ZIFs |
|
|
|
|
|
|
|
|
7373 |
64 |
NCNTs@MoS2 |
40 |
|
nm |
TEM |
nanotubes are uniform with a shell thickness of about 40nm |
22.605 |
|
|
|
|
|
|
|
7374 |
65 |
CuO NFs@MP |
20-40 |
|
nm |
TEM |
the CuO NFs@MP clearly indicated the deposition of CuO NFs with an average size of 20–40 nm |
20.88 |
|
|
|
|
|
|
|
7375 |
66 |
Fe3O4 NPs |
~11 |
|
nm |
TEM |
a granular shape with a mean size of ˜11 nm |
|
|
|
|
|
|
|
|
7376 |
68 |
Fe3O4@SiO2-NH2-Au@PdNPs |
<10 |
|
nm |
XRD |
The absorption spectrum of the AuNPs in Figure 1a-ii showed surface plasmon resonance (SPR) at 514 nm, and this is characteristic of small spherical nanoparticles with size less than 10 nm |
|
|
|
|
|
|
|
|
7377 |
71 |
Au/Co@HNCF |
|
|
|
|
|
|
|
|
|
|
|
|
|
7378 |
73 |
VOxNDs |
3.36 |
0.23 |
nm |
TEM |
lateral size |
|
|
|
|
|
|
|
|
7379 |
73 |
VOxNDs |
3.16 |
0.3 |
nm |
TEM |
the thicknesses |
|
|
|
|
|
|
|
|
7380 |
75 |
BDD|PB nanozymes |
|
|
|
SEM |
The average apparent doped-diamond grain size is between 50 and 500 nm |
|
|
|
|
|
|
|
|
7381 |
76 |
DNA-Ag/Pt NCs |
4 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7383 |
77 |
TPP-MoS2 QDs |
50 |
|
nm |
TEM |
the lateral diameters |
|
|
|
|
|
|
|
|
7382 |
77 |
TPP-MoS2 QDs |
1.69 |
0.15 |
nm |
TEM |
the thicknesses |
|
|
|
|
|
|
|
|
7384 |
78 |
AuNP |
38 |
|
nm |
TEM |
average diameter |
|
|
|
|
|
|
|
|
7385 |
81 |
Pt–Ni nanoparticles |
|
|
|
|
|
|
|
|
|
|
|
|
|
7386 |
82 |
PNCNzyme |
100 |
10 |
nm |
TEM |
uniform size of approximately 100 ± 10 nm in diameterwith hollow and porous structure |
|
|
|
|
|
|
|
|
7387 |
84 |
Co-V MMO nanowires |
|
|
|
|
|
33.63 |
|
|
|
|
|
|
|
7388 |
85 |
Pt@P-MOF(Fe) |
500 |
|
nm |
SEM |
the ellipsoidal morphology with a uniform size of 500 nm |
|
|
|
|
|
|
|
|
7390 |
87 |
CeM |
|
|
|
|
|
|
|
|
|
7 |
4 |
U/mg |
|
7389 |
87 |
CeM |
|
|
|
|
|
|
|
|
|
7 |
2 |
U/mg |
|
7392 |
90 |
nitrogen and sulfur codoped graphene (NSG) |
|
|
|
|
|
|
|
|
|
|
|
|
|
7393 |
90 |
graphene oxide (GO) |
|
|
|
|
|
|
|
|
|
|
|
|
|
7391 |
90 |
nitrogen doped graphene (NG) |
|
|
|
|
|
|
|
|
|
|
|
|
|
7394 |
91 |
Au@AgPt |
300 |
30 |
nm |
SEM |
Fig. 2a shows the SEM image of the as-synthesized Au NPs. The Au NPs exhibit hexoctahedral profiles with edge length of 90± 5 nm and diameter of 300±30 nm |
|
|
|
|
|
|
|
|
7396 |
92 |
Rhodium |
16.3 |
|
nm |
DLS |
The average hydrodynamic size of Rh-PEG NDs was ∼16.3 nm as determined by dynamic light scattering (DLS) |
|
|
|
|
|
|
|
|
7395 |
92 |
Rhodium |
5 |
|
nm |
TEM |
Fig.1a |
|
|
|
|
|
|
|
|
7397 |
94 |
Cu2+-catecholamines incorporated nanoflowers |
|
|
|
|
|
|
|
|
|
|
|
|
|
7398 |
95 |
Co3O4 |
210 |
|
nm |
TEM |
The transmission electron microscopy (TEM) images of the as-prepared Co3O4 MNE are shown in Figure 1A, which has a flower-like shape with an average size of ≈210 nm. |
|
|
|
|
|
|
|
|
7399 |
96 |
AuNCs |
1.77 |
|
nm |
TEM |
The TEM image showed that the obtained AuNCs-Apt was pseudo spherical particles with the average size of 1.86 nm (Fig. 1B and D), which was a little larger than that of bare AuNCs (1.77 nm) (Fig. 1A and C). |
|
|
|
|
|
|
|
|
7400 |
97 |
Prussian Blue |
49 |
|
nm |
Others |
Prussian Blue nanoparticles with Ø =49nm were used |
|
|
|
|
|
|
|
|
7401 |
98 |
Tb-OBBA-Hemin |
200-1500 |
|
nm |
SEM |
As shown in Figure 1a, the as-prepared Tb-OBBA-Hemin has spherical particles with a size of 200 nm to 1.5 μm |
21.38 |
|
|
|
|
|
|
|
7402 |
101 |
CeO2 NPs |
<10 |
|
nm |
TEM |
The particle is negatively charged with an average diameter less than 10 nm |
|
|
|
|
|
|
|
|
7403 |
103 |
CeO2NRs-MOF |
120 |
|
nm |
TEM |
the length of the prepared CeO2NRs is about 120 nm |
|
|
|
|
|
|
|
|
7404 |
105 |
AU-1 |
|
|
|
|
|
|
|
|
|
|
|
|
|
7405 |
106 |
IMSN-PEG-TI |
100 |
|
nm |
TEM |
The typical transmission electron microscopy (TEM) and scanning electron microscopy (SEM) images indicated the as-prepared IMSN exhibited a uniform spherical morphology with an average diameter of about100 nm, and the surface of IMSN became rough (Figure 1b,c). |
|
|
|
|
|
|
|
|
7406 |
108 |
HP-MIL-88B-BA |
|
|
|
|
|
|
|
|
|
|
|
|
|
7407 |
109 |
IrOx |
~24.05 |
|
nm |
TEM |
The as-prepared nanoparticles show a spherica morphology with diameter of ~24.05±0.29 nm (Figure 1b) |
|
|
|
|
|
|
|
|
7408 |
110 |
SnSe |
|
|
|
|
|
|
|
|
|
|
|
|
|
7409 |
111 |
F-BS NCs |
|
|
nm |
TEM |
BSA-capped Fe3O4@Bi2S3nanocatalysts (F-BSP NCs) dispersed well and stably in the DMEM medium (Figure S6) with an average hydrodynamic size of around 342 nm but with 396 nm in both water and PBS (Figure S7B). |
|
|
|
|
|
|
|
|
7410 |
112 |
Cerium Oxide Nanoparticles |
|
|
|
|
|
|
|
|
|
|
|
|
|
7411 |
113 |
PB |
|
|
|
|
|
|
|
|
|
|
|
|
|
7412 |
114 |
Pt-carbon nanozyme |
122 |
|
nm |
DLS |
The DLS analysis showed that the particle size of Pt-carbon nanozymes was approximately 122 nm. |
|
|
|
|
|
|
|
|
7413 |
115 |
CuO-C-dots |
|
|
|
TEM |
well-dispersed C-dots were of uniform (small spherical) shape with an average diameter of 2 nm |
|
|
|
|
|
|
|
|
7414 |
117 |
Au/Fe-MOF |
300 |
2.6 |
nm |
TEM |
average size of Fe-MOF is about 300 ± 2.6 nm. there are many uniformLy distributed small particles which are approximately 7 nm in diameter on the Fe-MOF surface after the reduction of HAuCl4. |
|
|
|
|
|
|
|
|
7415 |
118 |
Au@Au-aptamer |
12 |
|
nm |
DLS |
|
|
|
|
|
|
|
|
|
7416 |
119 |
ZIF-67 |
400 |
|
nm |
SEM |
|
1833.26 m2/g |
|
|
|
|
|
|
|
7417 |
120 |
Fe3O4-Au@Ag |
400 |
|
nm |
TEM |
The diameter of the AuNPs was about 2.7 nm. The particle size of Au@Ag NPs increased to about 8 nm.The Fe3O4 MNPs exhibited a spherical morphology with approximately 400 nm in diameter. |
|
|
|
|
|
|
|
|
7418 |
121 |
CeO2/C nanowires |
3-6 |
|
μm |
SEM |
the CeO2 NPs with mean size of about 6.83 nm are dispersed in the CeO2/C nanowire frameworks |
|
|
|
|
|
|
|
|
7419 |
122 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
7420 |
123 |
Cu‐HNCS |
390 |
|
nm |
TEM |
Cu‐HNCS with an average planar dimension of ≈390 nm and a wall thickness of ≈20 nm |
|
|
|
|
|
|
|
|
7421 |
124 |
PPy@MnO2-BSA |
15 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7422 |
125 |
Ag@Au core/shell TNPs |
|
|
|
|
gold shells of different thickness were deposited on the Ag TNPs by controlling the amount of HAuCl4 |
|
|
|
|
|
|
|
|
7423 |
126 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
7424 |
127 |
GOx-MnO2/HMME |
200 |
|
nm |
SEM |
the average pore diameter was about 3.85 nm |
50.34 m2/g |
|
|
|
|
|
|
|
7425 |
128 |
BNS-CDs |
2.2 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7426 |
129 |
CoFe-LDH/CeO2 |
|
|
|
|
CeO2 NTs were composed of numerous nanoparticles with grain size of 10-30 nm. |
35.7 m2/g |
|
|
|
|
|
|
|
7427 |
130 |
Ru4PCVs |
25 |
15 |
μm |
DLS |
|
|
|
|
|
|
|
|
|
7428 |
134 |
CTF–1 |
|
|
|
|
The SEM and TEM images shown in Fig. 1c and d indicates that CTF–1 has a layered–like structure. |
|
|
|
|
|
|
|
|
7429 |
137 |
Zr-MOF |
60 |
|
nm |
SEM |
As demonstrated by Fig. 1C, the synthesized Zr-MOF presents a uniform spherical morphology, and the diameter is ∼60 nm. |
217.5 |
|
|
|
|
|
|
|
7430 |
138 |
Ru@CeO2 YSNs |
78 |
|
nm |
DLS |
The hydrated particle size distribution indicates that the size of Ru@CeO2 YSNs were approximately 78 nm, |
81.3 |
|
|
|
|
|
|
|
7431 |
139 |
AuNFs/Fe3O4@ZIF-8-MoS2 |
|
|
|
|
|
|
|
|
|
|
|
|
|
7432 |
140 |
Fe3+/AMP CPs |
100 |
|
nm |
TEM |
Under TEM an extended network structure composed of aggregated nanoparticles was observed (Fig. 1b), which should give a large surface area for reaction. The average feature size is about 100 nm (Fig. S1, Supporting Information). |
|
|
|
|
|
|
|
|
7433 |
141 |
CDAu |
|
|
|
|
|
|
|
|
|
|
|
|
|
7434 |
142 |
CDs |
5-10 |
|
nm |
TEM |
The representative transmission electron microscope (TEM) images showed that both l-CDs and d-CDs had a size distribution of 5–10 nm and clear crystalline cores (Figure S1 in the Supporting Information). |
|
|
|
|
|
|
|
|
7435 |
144 |
Au21Pd79 |
1-2 |
|
μm |
TEM |
|
|
|
|
|
|
|
|
|
7436 |
145 |
Ag/ZnMOF |
|
|
|
|
|
|
|
|
|
|
|
|
|
7437 |
147 |
Fe3O4@Cu/GMP |
>1 |
|
μm |
DLS |
Dynamic light scattering (DLS) (Helos-Sucell, Sympatec GmbH, Germany) showed that the average size of Cu/GMP and Fe3O4@Cu/GMP particles were over 1 μm, indicating agglomeration of Cu/GMP and Fe3O4@Cu/GMP, consistent with the above TEM data. |
|
|
|
|
|
|
|
|
7438 |
148 |
AgNP@CD |
30 |
|
nm |
AFM |
|
|
|
|
|
|
|
|
|
7439 |
149 |
NiO |
10-20 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7440 |
150 |
Co3O4@β-CD NPs |
10 |
|
nm |
TEM |
The morphology of Co3O4@β-CD NPs showed well dispersed nanoparticles in the size of 10 nm. |
|
|
|
|
|
|
|
|
7441 |
151 |
Hf-DBP-Fe |
82.1 |
2.1 |
nm |
DLS |
Dynamic light scattering (DLS) showed similar number-averaged sizes of 82.1 ± 2.1 for Hf-DBP-Fe and 81.6 ± 3.6 nm for Hf-DBP (Fig. 2d). |
|
|
|
|
|
|
|
|
7442 |
154 |
GOD/hPB@gellan |
|
|
|
|
|
|
|
|
|
|
|
|
|
7443 |
155 |
Au NCs-ICG |
~10 |
|
nm |
TEM |
After ICG loading, the hydrodynamic size of Au NCs-ICG nanozymes sequentially increased to ∼10 nm, |
|
|
|
|
|
|
|
|
7444 |
156 |
Au@NH2-MIL-125(Ti) |
<5 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7445 |
156 |
Au@NH2-MIL-125(Ti) |
300 |
|
nm |
SEM |
thickness |
|
|
|
|
|
|
|
|
7446 |
156 |
Au@NH2-MIL-125(Ti) |
500 |
|
nm |
SEM |
diameter |
|
|
|
|
|
|
|
|
7448 |
157 |
Bi2S3@DMSN |
110.6 |
18.6 |
nm |
TEM |
length |
|
|
|
|
|
|
|
|
7447 |
157 |
PEG/Ce-Bi@DMSN |
3-4 |
|
nm |
TEM |
The TEM image of the CeO2 nanozymes presented in Figure 1d, shows that the CeO2 nanozymes were 3–4 nm in diameter and were suitable for loading into the large-pore channels of Bi2S3@ DMSN nanoparticles |
|
|
|
|
|
|
|
|
7449 |
157 |
Bi2S3@DMSN |
65.6 |
9.2 |
nm |
TEM |
width |
201.32 |
|
|
|
|
|
|
|
7451 |
158 |
AgPd@BSA/DOX |
120 |
|
nm |
TEM |
Nevertheless, both Ag NPs and AgPd NPs have similar mean particle sizes overall about 120 nm |
|
|
|
|
|
|
|
|
7450 |
158 |
AgPd@BSA/DOX |
216 |
7.03 |
nm |
DLS |
As shown in Fig. 2k, the DLS results revealed that the hydrodynamic sizes of the Ag NPs, AgPd NPs, AgPd@BSA and AgPd@BSA/DOX were 158 ± 4.18, 165 ± 5.74, 214 ± 8.41, 216 ± 7.03 nm, respectively, which is bigger than actual size observed from the TEM image. |
|
|
|
|
|
|
|
|
7452 |
159 |
Au@Pt |
50 |
|
nm |
TEM |
A typical TEM image (Fig. 3) showed that the Au@Pt nanozymes were relatively uniform in size and similar in structure, and the diameter of the nanoparticles was approximately 50 nm. As a uniform porous structure, Pt NPs formed a branched structure on the surface ofAu. The particle size ofthe Au corewas approximately 30e35 nm, and the average diameter of the Pt NPs was approximately 5e10 nm. |
|
|
|
|
|
|
|
|
7453 |
160 |
Fe-N-C |
|
|
|
|
Thetransmission electron microscopy (TEM) images disclosed the onion-like nanoparticles of tens of nanometers with multiple graphitic shells and void cores for Fe-N-C-850 |
|
|
|
|
|
|
|
|
7454 |
161 |
CeO2/Mn3O4 Nanocrystals |
4 |
|
nm |
TEM |
Heterostructured CeO2/Mn3O4 nanocrystals were prepared by a seed-mediated growth process.[14] The seeds, 4 nm sized truncated octahedral CeO2 nanocrystals, predominantly enclosed by {100} and {111} (Figure 1a), were reacted with MnCl2 to yield the |
|
|
|
|
|
|
|
|
7455 |
162 |
Ir@MnFe2O4 NPs |
11.24 |
1.11 |
nm |
TEM |
The average sizes of the MnFe2O4 NPs and Ir@MnFe2O4 NPs were determined by manually counting to be 10.47 ± 0.99 nm and 11.24 ± 1.11 nm respectively |
|
|
|
|
|
|
|
|
7456 |
164 |
PBNPs in TiNM |
|
|
|
SEM |
the TiNM was composed of parallel nanochannels, and these nanochannels have conical shape with an average diameter of a large base entrance of -200 nm and small tip entrance of -50 nm |
|
|
|
|
|
|
|
|
7457 |
165 |
VONP-LPs |
25 |
1.5 |
nm |
TEM |
the particle size distribution of V2O5 NPs in the range of 15–40 nm with average lateral size of 25 � 1.5 nm. |
|
|
|
|
|
|
|
|
7458 |
166 |
CB-CQDs |
1.5-3.6 |
|
nm |
TEM |
They exhibit a size range of 1.5–3.6 nm with an average diameter of about 2.4 nm, fitting well to the Gaussian function |
|
|
|
|
|
|
|
|
7459 |
167 |
UsAuNPs/MOFs |
150 |
|
nm |
TEM |
The UsAuNPs/MOFs present uniform dispersion with an average size of around 150 nm (Figure S11, Supporting Information). |
|
|
|
|
|
|
|
|
7460 |
168 |
MIL-101(Fe) |
500 |
|
nm |
SEM |
SEM images showed that MIL-101(Fe) had the well-defined octahedral morphology with an average diagonal length of approximately 500 nm |
2702.9 |
|
|
|
|
|
|
|
7461 |
169 |
FeTPP assemblies within AuTTMA monolayer |
~2 |
|
nm |
Others |
In our previous studies, we incorporated hydrophobic TMCs into the monolayer of 2-nm gold nanoparticles (NPs),6,29–31 to generate nanozymes that were functional in complex biological environments |
|
|
|
|
|
|
|
|
7462 |
171 |
HS-PtNPs |
4.8 |
0.6 |
nm |
TEM |
TEM image shows that the average diameter of HS-PtNPs was 4.8 ± 0.6 nm (Fig. 1C), and the high resolution TEM (HRTEM) image shows that HS-PtNPs possessed a 0.30 nm continuous lattice spacing |
|
|
|
|
|
2819.16 |
U/g |
|
7463 |
172 |
Fe3O4@PDA@BSA-Bi2S3 |
120, 125, and 123 |
|
nm |
DLS |
The DLS size of Fe3O4@PDA@BSA-Bi2S3 NPs were indicated as 120, 125, and 123 nm, respectively, and showed no detectable fluctuation during the 5 days storage |
|
|
|
|
|
|
|
|
7464 |
173 |
MoO3 NPs |
2-4 |
|
nm |
TEM |
The TEM image in Fig. 1A shows that the MoO3 NPs are well dispersed with an average diameter of 2.0e4.0 nm. The lattice spacing of 0.21 nm in the HRTEM image |
|
|
|
|
|
|
|
|
7465 |
174 |
IrRu-GOx@PEG NPs |
43 |
|
nm |
TEM |
Therefore, we synthesized IrRu NPs with different ratio of Ir and Ru elements to obtain better enzyme-like catalytic activity. the TEM image showed Ir2Ru1 NPs, Ir4Ru1 NPs, and Ir8Ru1 NPs are uniformly dispersed black particles with an average particle size of ~2 nm (Fig. 1A and B) and ~3 nm (Figs. S1A and B), ~4 nm.As shown in TEM images, the IrRuGOx@PEG NPs obtained by PEG-coated IrRu NPs were spherical and the average particle size was ~43 nm |
|
|
|
|
|
|
|
|
7466 |
175 |
Fe3O4/CoFe-LDH |
320-350 |
|
nm |
TEM |
As displayed in Fig. 2a and b, Fe3O4 were well-separated lycheelike spherical structure with mean grain size of about 300 nm. Fig. 2c-e clearly show the core-shell structure where Fe3O4 microspheres were encapsulated in CoFe-LDH nanosheets. Since there were no obvious boundaries between the core and shell, we approximately estimated that the particle sizes of Fe3O4/CoFe-LDH were in the range of 320-350 nm |
44.5 |
|
|
|
|
|
|
|
7467 |
176 |
N-doped MoS2 |
|
|
|
|
|
|
|
|
|
|
|
|
|
7468 |
178 |
Au 1 Pd 5 |
1.4 |
|
nm |
TEM |
TEM was performed to investigate the size distribution of monometallic and bimetallic NCs. As shown in Fig. 2a and b, NADH-reduced Pd NCs with 24 h-incubation exhibit the mean size of 1.1 nm, while Au NPs show the average diameter of 8.1 nm. Remarkably, both Au1Pd5 and Au1Pd1 exist as highly dispersed NCs, showing the average size of 1.4 and 1.6 nm respectively (Fig. 2c and d). The mean size increases in the order of Pd < Au1Pd5 < Au1Pd1 < Au, which is consistent with the relative content of Au species. Hence, it is reasonable that NADH facilitates the rapid formation of ultrasmall NCs within a suitable range of [Na2PdCl4]/[HAuCl4]. Further, the atomic ratio in bimetallic NCs was determined by ICP-OES. The molar ratio of [Au]/[Pd] is 1.3 for Au1Pd1 and 0.25 for Au1Pd5, which is close to the corresponding theoretical ratio of two precursors in synthesis process. |
|
|
|
|
|
|
|
|
7469 |
179 |
PMOF(Fe) |
300 |
|
nm |
SEM |
The low-magnification SEM images revealed that PMOF(Fe) was of uniform ellipsoidal shape with an average diameter of 300 nm (Figure 1A). TEM images in Figure 1B further show the morphology and size of PMOF(Fe), which was consistent with the result of SEM. After modifying the Pt NPs on the surface of PMOF(Fe), Pt@PMOF(Fe) kept the morphology of PMOF(Fe) (Figure 1C) and with a lot of Pt NPs. The size of Pt NPs is around 2 nm (Figure 1D, inset). These Pt NPs were modified on the surface of PMOF(Fe) uniformly. |
|
|
|
|
|
|
|
|
7470 |
181 |
hemin@CD |
2.3 |
|
nm |
TEM |
High-resolution TEM image shows the lattice fringe of 0.21 nm corresponding to the (100) facet (inset of Fig. 1a) [27]. After hemin was modified on CDs, the average size of hemin@CDs is 2.3 nm (Fig. 1b), which suggests there have been no significant change in the average size of CDs after hemin molecule decoration. |
|
|
|
|
|
|
|
|
7471 |
182 |
T-BiO2–x NSs |
150 |
|
nm |
DLS |
The mean hydrodynamic size of T-BiO2–x NSs is around 150 nm |
|
|
|
|
|
|
|
|
7472 |
183 |
GCE/MWCNTs-Av/RunNPs |
|
|
|
|
|
|
|
|
|
|
|
|
|
7474 |
184 |
GO–PtNPs |
|
|
nm |
TEM |
the TEM and STEM images of the formed GO/DNA–PtNPs showed sparsely distributed PtNPs with smaller size (1–2 nm) |
|
|
|
|
|
|
|
|
7473 |
184 |
GO–PtNPs |
6 |
|
nm |
TEM |
average size |
|
|
|
|
|
|
|
|
7475 |
186 |
mGPB |
~182 |
|
nm |
TEM |
After loading, the hydrodynamic size of the nanoparticles (162.2 nm) increased to ∼182.0 nm |
|
|
|
|
|
|
|
|
7476 |
189 |
CC-PdNPs |
2.4-2.7 |
|
nm |
TEM |
To determine a reliable size distribution, we carried out a statistical analysis by Gaussian fitting of 50 random nanoparticles according to TEM results and found that the diameters of PdNPs are mainly distributed in the 2.4–2.7 nm range with an average size of 2.68 nm |
|
|
|
|
|
|
|
|
7477 |
190 |
MNET |
216 |
|
nm |
TEM |
Meanwhile, the hydrodynamic dimension of Mn3O4 NPs was 25.5 ± 3 nm by DLS (Figure 1C). After Mn3O4 encapsulated, the average size of MNET increased from 186 to 216 nm |
|
|
|
|
|
|
|
|
7478 |
193 |
Cu-hNFs |
19 |
|
μm |
SEM |
Also, with SEM images, the diameter of Cu-NFs composed of nano-sized petals was measured as 19 µm. |
|
|
|
|
|
|
|
|
7479 |
194 |
aptamer-AuNPs |
18 |
|
nm |
DLS |
DLS is an effective method to measure the overall particle size distribution of nanomaterials. As can be seen from Fig. 3, the particle size of aptamer-AuNPs is about 18 nm with a small distribution range. |
|
|
|
|
|
|
|
|
7480 |
195 |
CDs@Cu4O3 |
|
|
|
|
|
|
|
|
|
|
|
|
|
7481 |
198 |
CuS |
180 |
|
nm |
SEM |
the morphology of CuS is hexahedrons with the size range of 118–238 nm and with an average size of 180 nm (Fig. S1) |
|
|
|
|
|
|
|
|
7483 |
199 |
M/H-D |
213.2 |
15.8 |
nm |
DLS |
After the modification of dextran, dynamic light scattering (DLS) measurements showed the average hydrous dynamic diameter of 70% of the M/H-D was ∼213.2 ± 15.8 nm (Figure S2). |
|
|
|
|
|
|
|
|
7484 |
199 |
HfO2 NPs |
2~5 |
|
nm |
TEM |
The size of HfO2 NPs (2–5 nm) anchored on the surface of MoS2 was smaller than the HfO2 NPs alone (10 nm), which could be attributed to the two different nucleation centers of HfO2 in the presence or absence of MoS2 NSs in the solution. |
|
|
|
|
|
|
|
|
7485 |
199 |
HfO2 NPs |
10 |
|
nm |
TEM |
The size of HfO2 NPs (2–5 nm) anchored on the surface of MoS2 was smaller than the HfO2 NPs alone (10 nm), which could be attributed to the two different nucleation centers of HfO2 in the presence or absence of MoS2 NSs in the solution. |
|
|
|
|
|
|
|
|
7482 |
199 |
MoS2 |
100-200 |
|
nm |
TEM |
a layered structure with approximately average size (the longest part) of 100–200 nm and uniform edges. |
|
|
|
|
|
|
|
|
7486 |
200 |
GeO2 |
|
|
|
|
showed besom-like morphology with uniform size (width of ≈100 nm and length of ≈1 µm). the “head of besom” was composed of long strip with width of ≈10 nm (Figure 1c,d). |
|
|
|
|
|
|
|
|
7487 |
201 |
CuS NPs |
7 |
|
nm |
TEM |
the carboxylic acid-stabilized CuS NPs were synthesized with an average size of approximately 7 nm. |
138.62 |
|
|
|
|
|
|
|
7488 |
202 |
Pt/EMT |
|
|
|
|
The EMT zeolite synthesized under mild conditions comprises a great number of uniform nanocrystals with slightly different morphology and average particle size of 15–20 nm (Fig. 2A and S2), in agreement with the result calculated by Scherrer Equation. Moreover, some highly-dispersed Pt NPs in size of 5–8 nm are confined within the zeolite (Fig. 2D) |
457 |
|
|
|
|
|
|
|
7489 |
203 |
Au nanoparticles (NPs) modified by cyclodextrin (Au@CD) |
20 |
|
nm |
|
As shown in Figure 2A, the Au@CD NPs showed good dispersity with a diameter around 20 nm. |
|
|
|
|
|
|
|
|
7490 |
205 |
rosette-GCN |
2.53 |
0.78 |
μm |
SEM |
The size of rosette-GCN was estimated to be 2.53 ± 0.78 μM through 20 times measurements in its SEM images. |
77.800 ± 0.669 |
|
|
|
|
|
|
|
7491 |
206 |
Au-nanozyme |
10 |
|
nm |
TEM |
the size distribution of Au-nanozyme was in the range of 3.0–30.3 nm and the average size of the nanoparticles was about 10 nm. |
|
|
|
|
|
|
|
|
7492 |
208 |
AgNPs |
7.4 |
|
nm |
TEM |
Figure S1 shows the TEM image of the resulting AgNPs, which reveals that the average size of AgNPs is about 7.4 nm. |
|
|
|
|
|
|
|
silver nanoparticles (AgNPs) display oxidase-like activity in the presence of Cl– as a cofactor |
7493 |
209 |
BSA-RuO2NPs |
7 |
|
nm |
TEM |
As can be seen in Figure 1C, size distribution analysis of 100 random BSA-RuO2NPs by Gaussian fitting, the particle size has been calculated to be ∼7 nm. |
|
|
|
|
710 |
|
U/g |
|
7494 |
210 |
AuNPs |
10 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7495 |
210 |
iron-based MOFs (IM) |
|
|
|
|
an average diameter and length around 60 and 400 nm respectively |
|
|
|
|
|
|
|
|
7496 |
212 |
MoOx QDs |
3.42 |
|
nm |
TEM |
As depicted in TEM images, the obtained MoOx QDs are highly uniform and monodisperse nanocrystals with the average size about 3.42 nm. |
|
|
|
|
|
|
|
|
7497 |
215 |
hydrogel |
50-70 |
|
nm |
|
As shown in Fig. 1(a), the hydrogel appeared to be a network nanofiber with diameters of 50–70 nm. |
2.318 |
|
|
|
|
|
|
|
7498 |
216 |
GO |
|
|
|
TEM |
|
|
|
|
|
|
|
|
|
7499 |
217 |
IrO2 |
1.7 |
0.3 |
nm |
DLS |
The average size of IrO2 nanoparticles was 1.7 ± 0.3 nm by counting more than 200 nanoparticles. The monodisperse IrO2 nanoparticles on GO indicated that GO had effectively inhibited the aggregation of IrO2 nanoparticles. There were no unsupported IrO2 nanoparticles observed, which indicated that the GO was an excellent support. |
|
|
|
|
|
|
|
|
7500 |
221 |
VB2-IONzymes |
<200 |
|
nm |
SEM |
The naked IONzymes showed a spherical shape with a diameter of about 200 nm. VB2-IONzymes became smaller and developed a rough surfaceupon modification with a high amount of VB2. |
|
|
|
|
|
|
|
|
7501 |
222 |
Hg2+/heparin–OsNPs |
|
|
|
|
|
|
|
|
|
81 |
|
U/g |
|
7502 |
222 |
Hg2+/heparin–OsNPs |
|
|
|
|
|
|
|
|
|
80.97 |
|
U/g |
TEM image of heparin–OsNPs. Inset: HRTEM image and the size distribution of heparin–OsNPs determined from the TEM image (from size distribution analysis of 50 random nanoparticles by Gaussian fitting). |
7503 |
223 |
laccase@MMOFs |
<100 |
|
nm |
SEM |
The laccase@MMOFs found spherical in nature with an average particle size below 100 nm |
343.27 |
|
|
|
|
|
|
|
7504 |
224 |
oxidized UiO-66(Ce/Zr) |
|
|
|
|
|
|
|
|
|
|
|
|
Correspondingly, the strong adsorption of Pi onto oxidized UiO-66(Ce/Zr) decreases the specific surface area and pore size of the latter |
7505 |
226 |
Pt NPs |
30 |
4 |
nm |
DLS |
The PtNPs were well monodispersed and displayed a uniform spherical shape with rough surfaces. Most of them were distributed in 30 ± 4 nm by randomly analyzing 200 particles (Figure S6). |
|
|
|
|
|
|
|
|
7506 |
227 |
Fe SSN |
|
|
|
|
|
578 |
|
|
|
|
|
|
|
7507 |
229 |
lipase immobilized on Fe3O4/SiO2/Gr NC |
|
|
|
SEM |
The morphology and structure of the Fe3O4/SiO2/Gr NC were revealed through the SEM microphotographs. It reveals the SEM visual of the as-synthesized Fe3O4/SiO2 having a blockish like structure over Gr nanostructured sheet (Fig. 2). |
|
|
|
|
|
|
|
|
7508 |
230 |
HP-HIONs@PDA-PEG |
526.24 |
48.89 |
nm |
TEM |
The diameter of the HP-HIONs@PDA-PEG was 526.24 ± 48.89 nm, as determined by TEM, corresponding to the results of DLS experiments (Fig. S1A, 588 ± 140.23 nm). |
|
|
|
|
|
|
|
|
7509 |
231 |
HKUST-1 |
85 |
|
nm |
TEM |
And the obtained HKUST-1 with blue color shows a regular sphere morphology with the average particle size of ∼85 nm in TEM imaging (Figure 1a) and a larger value of 140 nm in the DLS dispersed in water (Figure 1b). |
|
|
|
|
|
|
|
|
7510 |
232 |
AuPtRu |
200 |
|
nm |
TEM |
Transmission electron microscopy (TEM) imaging was performed to confirm the successful synthesis of AuPd, AuPt, and AuPtRu. As shown in Fig. 1a–c, AuPd, AuPt, and AuPtRu with the average sizes of 5, 4, and 200 nm were obtained, respectively. |
|
|
|
|
|
|
|
|
7511 |
234 |
CdCo2O4 |
|
|
|
|
|
72 |
|
|
|
|
|
|
The pore size analysis for adsorption data, based on the Barrett-Joyner-Halenda (BJH) theories, clearly indicates that the fabricated nanosheets possess pores with an average diameter of 20 nm |
7512 |
235 |
GOx&PVI-Hemin@ZIF-8 |
270 |
|
nm |
TEM |
The TEM image in Figure 1d displays a typical GOx&PVI-hemin@ZIF-8 particle with a diameter of ca. 270 nm. |
|
|
|
|
|
|
|
Compared to pure ZIF-8, the GOx&PVI-hemin@ ZIF-8 composite shows an obvious decrement of the Brunauer−Emmett−Teller surface areas, attributed to the encapsulation of nonporous GOx&PVI-hemin. |
7513 |
257 |
TiO2/C-QDs |
5.23 |
0.3 |
nm |
TEM |
The mean size was 5.23 nm, as calculated from 100 particlesin the TEM image. |
|
|
|
|
|
|
|
|
7514 |
258 |
RBIR |
3.5 |
|
nm |
TEM |
RBIR appeared as well-dispersed nanodots with |