7384 |
78 |
AuNP |
38 |
|
nm |
TEM |
average diameter |
|
|
|
|
|
|
|
|
7395 |
92 |
Rhodium |
5 |
|
nm |
TEM |
Fig.1a |
|
|
|
|
|
|
|
|
7396 |
92 |
Rhodium |
16.3 |
|
nm |
DLS |
The average hydrodynamic size of Rh-PEG NDs was ∼16.3 nm as determined by dynamic light scattering (DLS) |
|
|
|
|
|
|
|
|
7399 |
96 |
AuNCs |
1.77 |
|
nm |
TEM |
The TEM image showed that the obtained AuNCs-Apt was pseudo spherical particles with the average size of 1.86 nm (Fig. 1B and D), which was a little larger than that of bare AuNCs (1.77 nm) (Fig. 1A and C). |
|
|
|
|
|
|
|
|
7435 |
144 |
Au21Pd79 |
1-2 |
|
μm |
TEM |
|
|
|
|
|
|
|
|
|
7443 |
155 |
Au NCs-ICG |
~10 |
|
nm |
TEM |
After ICG loading, the hydrodynamic size of Au NCs-ICG nanozymes sequentially increased to ∼10 nm, |
|
|
|
|
|
|
|
|
7462 |
171 |
HS-PtNPs |
4.8 |
0.6 |
nm |
TEM |
TEM image shows that the average diameter of HS-PtNPs was 4.8 ± 0.6 nm (Fig. 1C), and the high resolution TEM (HRTEM) image shows that HS-PtNPs possessed a 0.30 nm continuous lattice spacing |
|
|
|
|
|
2819.16 |
U/g |
|
7491 |
206 |
Au-nanozyme |
10 |
|
nm |
TEM |
the size distribution of Au-nanozyme was in the range of 3.0–30.3 nm and the average size of the nanoparticles was about 10 nm. |
|
|
|
|
|
|
|
|
7492 |
208 |
AgNPs |
7.4 |
|
nm |
TEM |
Figure S1 shows the TEM image of the resulting AgNPs, which reveals that the average size of AgNPs is about 7.4 nm. |
|
|
|
|
|
|
|
silver nanoparticles (AgNPs) display oxidase-like activity in the presence of Cl– as a cofactor |
7505 |
226 |
Pt NPs |
30 |
4 |
nm |
DLS |
The PtNPs were well monodispersed and displayed a uniform spherical shape with rough surfaces. Most of them were distributed in 30 ± 4 nm by randomly analyzing 200 particles (Figure S6). |
|
|
|
|
|
|
|
|
7515 |
259 |
Pd8 |
8.34 |
1.17 |
nm |
TEM |
|
|
|
|
|
|
|
|
|
7516 |
259 |
Pd4 |
4.18 |
0.82 |
nm |
TEM |
|
|
|
|
|
|
|
|
|
7517 |
260 |
PtNPs |
4.17 |
|
nm |
TEM |
the PtNPs with an average diameter of 4.17 nm were largely monodisperse. |
|
|
|
|
|
|
|
|
7531 |
273 |
PtGs |
136 |
|
nm |
DLS |
|
|
|
|
|
|
|
|
|
7539 |
292 |
RuTeNRs |
|
|
|
TEM |
According to transmission electron microscopy (TEM) images, hollow nanorods with lengths of 130 ± 13 nm and widths of 14 ± 2 nm (n = 30) were synthesized with a relatively monodisperse distribution (Figure 2a; left) |
|
|
|
|
|
|
|
|
7565 |
324 |
Cu NCs |
2.5 |
|
nm |
TEM |
The as-prepared Cu NCs were approximately 2.5 nm in diameter |
|
|
|
|
|
|
|
|
7574 |
336 |
AuNPs |
~13-20 |
|
nm |
Others |
|
|
|
|
|
|
|
|
|
7577 |
338 |
Pt@Au |
121.6 |
10.7 |
nm |
TEM |
|
|
|
|
|
|
|
|
|
7578 |
338 |
Pt@Au |
159.6 |
7.7 |
nm |
DLS |
|
|
|
|
|
|
|
|
|
7581 |
339 |
AuNRs@CTAB treated with Ag+ ion |
55 |
|
nm |
DLS |
the average hydrodynamic diameters |
|
|
|
|
|
|
|
|
7579 |
339 |
AuNCs@CTAB treated with Ag+ ion |
68 |
|
nm |
DLS |
|
|
|
|
|
|
|
|
|
7580 |
339 |
AuNSs@CTAB treated with Ag+ ion |
60 |
|
nm |
DLS |
|
|
|
|
|
|
|
|
|
7582 |
340 |
AuNPs |
16 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7593 |
353 |
Au@Pt NP |
30 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7595 |
357 |
PtNFs |
51.1 |
3.1 |
nm |
TEM |
the nanoparticles display a uniform hydrangea-like shape with a size of about 51.1 ± 3.1 nm. |
|
|
|
|
|
|
|
|
7597 |
359 |
CPT-TK-HPPH/Pt NP |
100 |
|
nm |
TEM |
The TEM imaging, shown in Figure 2A, revealed that the CPT-TK-HPPH/Pt NP had a uniform size of ≈100 nm |
|
|
|
|
|
|
|
|
7598 |
359 |
CPT-TK-HPPH/Pt NP |
179.67 |
2.45 |
nm |
DLS |
The hydrodynamic diameter and zeta potential of CPT-TK-HPPH/Pt NP were 179 nm (PDI = 0.207) and −40 mV, respectively. |
|
|
|
|
|
|
|
|
7599 |
360 |
curcumin based Cu-hNs |
19-36 |
|
μm |
SEM |
The characterization datas confirm that curcumin based Cu-hNs have between 19 and 36 μm diameter and synthesized in PBS buffer. |
|
|
|
|
|
|
|
|
7601 |
362 |
Aptamer-gold nanozyme |
21 |
|
nm |
DLS |
the average diameter of AuNPs to be ~10 nm .The absorption maxima of AuNPs after conjugation shifted from 521 nm to 530 nm (Fig. 2A) and particle size increases from 10 nm to 21 nm was observed (Fig. 2B and C). |
|
|
|
|
|
|
|
|
7605 |
366 |
Pd−Ir core-shell nanoparticles |
3.3–13.0 |
|
nm |
TEM |
Pd−Ir nanoparticles with four different sizes (3.3, 5.9, 9.8 and 13.0 nm), but identical shapes and surface structures, were designed and synthesized. |
|
|
|
|
|
|
|
atalytic activity of individual Pd−Ir NPs increases as particle size increases. Area-specific catalytic activity is similar for Pd−Ir NPs of 3.3–9.8 nm, but is slightly decreased when particle size reached to 13.0 nm. |
7617 |
383 |
AuNPs@Ag |
24.4 |
|
nm |
DLS |
The hydrodynamic size of AuNPs were found 13.66 ± 3.66 nm with polydispersity index of 0.273 which increased to 24.4 nm after the Ag deposition, measured by DLS |
|
|
|
|
|
|
|
|
7624 |
386 |
PEI-AgNCs |
2~5 |
|
nm |
TEM |
well-dispersed Ag nanoclusters are gained, and the size of these clusters is in the range of2~5 nm |
|
|
|
|
|
|
|
|
7639 |
401 |
Exo@Au |
2,8,13,30,60 |
|
nm |
TEM |
5 kind of Au NPS |
|
|
|
|
|
|
|
|
7641 |
407 |
AuNPs |
20 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7667 |
436 |
MPBs |
54.1 |
6.9 |
nm |
TEM |
The diameter was increased to approximately 81.3 ± 3.5 nm from 54.1 ± 6.9 nm and part of the microchannel was also filled after incorporation of PB with MSNs, as observed by SEM and TEM |
633.91 |
|
|
|
|
|
|
|
7668 |
437 |
Au NP |
13 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
7689 |
454 |
Au NPs |
14.4 |
1.8 |
nm |
TEM |
The TEM images showed that Au NPs are homogeneous with a diameter of 14.4 ± 1.8 nm as measured by ImageJ (n = 90) (Figure 2a). |
|
|
|
|
|
|
|
|
7700 |
466 |
4-AHA@AuNPs nanoparticles |
5.9 |
1.7 |
nm |
TEM |
The produced nanoparticles were quasi-spherical in shape with average particle size of about 5.9 ± 1.7 nm [Fig. 2b]. |
|
|
|
|
|
|
|
|
7741 |
509 |
AuNPs@C.CNF |
12 |
3 |
nm |
DLS |
The synthesis process was further monitored by changing the MW irradiation time (5–35 s) at a fixed concentration of C.CNF (1.0 %),12 ± 3 nm (1.0 % C.CNF) |
|
|
|
|
|
|
|
|
7744 |
513 |
FA-AgNPs |
20 |
|
nm |
TEM |
From transmission electron microscopy (TEM), the particles were roughly spherical with uniformed size (Fig. 1A). |
|
|
|
|
|
|
|
|
7745 |
515 |
aptamers@BSA-AuNCs |
1.77 |
0.51 |
nm |
TEM |
The average diameters of BSA-AuNCs and aptamers@BSA-AuNCs are 1.79 ± 0.52 nm and 1.77 ± 0.51 nm, respectively (Figs. S2B and S2D). |
|
|
|
|
|
|
|
|
7748 |
518 |
Hep-Pt NCs |
1.5-2.1 |
|
nm |
TEM |
As the molar ratio of [K2PtCl4]/[Hep] increases from 0.2 to 3, the mean size of gradually grows from 1.5 to 2.1 nm. |
|
|
|
|
|
|
|
|
7771 |
543 |
Au@SiO2-NH2 |
130 |
2.3 |
nm |
DLS |
|
|
|
|
|
|
|
|
|
7780 |
549 |
β-CD@AuNPs |
50 |
|
nm |
TEM&SEM |
|
|
|
|
|
|
|
|
|
7791 |
561 |
urchin-like Pt nanozymes |
40 |
|
nm |
TEM |
Figure 2A shows well synthesized Pt seeds with a diameter of ~5 nm. uPtNZs exhibited fairly uniform dispersion with a mean diameter of ~40 nm in TEM images (Fig. 2B) |
|
|
|
|
|
|
|
|
7797 |
569 |
Au NPs |
23 |
4 |
nm |
TEM |
The TEM imaging, absorbance, and fluorescence spectra revealed the consistent average size of the Au-NPs ∼23 ± 4 nm, while the DLS measurements 64 resulted in their hydrodynamic diameter ∼39 ± 4 nm, which is an expected difference from the size reported by other methods. |
|
|
|
|
|
|
|
|
7862 |
644 |
Pt |
80 |
|
nm |
TEM |
Average |
|
|
|
|
|
|
|
|
7864 |
646 |
Co(OH)2 |
500 |
|
nm |
TEM |
Average |
|
|
|
|
|
|
|
|
7867 |
649 |
Iron-based NPs |
|
|
|
|
|
|
|
|
|
|
|
|
|
7874 |
658 |
AuNPs |
|
|
|
|
|
|
|
|
|
|
|
|
|
7883 |
666 |
AuNCs-SF |
|
|
|
SEM |
|
|
|
|
|
|
|
|
|
7885 |
668 |
D-Trp-OMe@AuNCs |
2.3 |
|
nm |
DLS |
As shown in Fig. 2a and b, the D-Trp-OMe@AuNCs were monodisperse and spherical with an average size of 2.3 nm. The addition of TC induced the aggregation of D-Trp-OMe@AuNCs to form the D-Trp-OMe@AuNCs-TC composites [28] (Fig. 2d). Fig. 2c clearly shows that 24.2 nm was the average size of the D-Trp-OMe@AuNCs-TC composites. |
|
|
|
|
|
|
|
|
7888 |
671 |
IrNPs |
90 |
|
nm |
TEM |
The transmission electron microscopy (TEM) image of IrNPs shows particles with a rough surface morphology and a transverse diameter of ∼90 nm (Figure 2a). |
|
|
|
|
|
|
|
|
7909 |
695 |
Pt |
30 |
|
nm |
TEM |
As shown in Figure 1a, the prepared Pt NPs were about 30 nm and formed by these so-called “building blocks” with a size of 5 nm |
|
|
|
|
|
|
|
|
7919 |
707 |
AuNPs |
|
|
|
|
|
|
|
|
|
|
|
|
|
7937 |
727 |
Ir NPs |
~2.4 |
|
nm |
TEM |
Transmission electron microscopy (TEM) images indicated that the as-prepared Ir NPs showed a narrow size distribution with the average diameter of ∼2.4 nm (Fig. 1A–C). |
|
|
|
|
|
|
|
|
7965 |
754 |
Pt nanocrystals |
1-4 |
|
nm |
DLS |
Moreover, Pt NPs prepared with CMP exhibit larger particle sizes than those prepared with GMP (Fig. 2a–d). The average diameter of asprepared Pt NPs decreases in the following order: Pt-CMP/EG (3.4 nm) > Pt-GMP/EG (2.2 nm) > Pt-CMP/H2O (1.9 nm) > Pt-GMP/H2O (1.2 nm). This order of size distribution was further verified by DLS |
|
|
|
|
|
|
|
|
7977 |
771 |
Au NPS |
2.2 |
0.4 |
nm |
TEM |
|
|
|
|
|
|
|
|
|
7999 |
788 |
AuNPTs |
|
|
nm |
SEM |
AuNPTs, triangular plates with an average side-length of about 132 nm and a thickness of about 10 nm |
|
|
|
|
|
|
|
|
8005 |
794 |
PB |
34 |
8 |
nm |
DLS |
The PB nanozyme exhibited an average hydrodynamic size of 34 ± 8 nm with a good monodispersity (polydispersity index ~0.2) in DLS analysis (Fig. 1b). |
|
|
|
|
|
|
|
|
8012 |
803 |
PtNP |
30 |
|
nm |
|
As depicted in Figure 2 a, nonfaradaic capacitive currents were mainly observed at indium tin oxide (ITO) electrodes in tris buffer (pH 9.0) containing 4-aminonaphthalene-1-yl acetate (1), 1 and AB, and 1 and platinum nanoparticle (PtNP, 30 nm in diameter) after an incubation period of 10 min (curves i-iii of Figure 2 a). |
|
|
|
|
|
|
|
|
8014 |
807 |
AuNPs |
25 |
|
nm |
TEM |
The morphology of the His-AuNCs was studied via their TEM images taken. As sit is seen from Fig. 1A, the average diameter of the synthesized His-AuNCs is about 2 nm and their morphology and size are nearly spherical and uniform. The TEM images were also utilized to estimate the average diameters of the enlarged AuNPs seeds in the presence of glucose (Fig. 1B). The average diameters of His-AuNPs seeds were 10 ± 2 nm, while the diameter of enlarged AuNPs depend on the concentration of glucose and self-catalyzed activity of AuNPs. The TEM images reveal that the AuNPs in the presence of 50 μM glucose can be enlarged to an average size of 17 nm (Fig. 1C), while the diameter of enlarged AuNPs in the presence of higher glucose concentrations of 100 μM further increased to about 25 nm (Fig. 1D). |
|
|
|
|
|
|
|
|
8016 |
810 |
GOx@Au@MagSiO2 |
6.5 |
|
μm |
SEM |
The mean particle size and coefficient of variation for size distribution were calculated as 6.5 μm and 4.1%, respectively (Fig. 3A and Table 1). |
12.3 |
|
|
|
|
|
|
|
8017 |
812 |
Cu NCs |
1.7 |
0.1 |
nm |
TEM |
The TEM image of as-synthesized Cu NCs clearly shows the formation of spherical and well-dispersed particles with an average diameter of 1.7 ± 0.1 nm (Figure 2A). |
|
|
|
|
|
|
|
|
8024 |
821 |
[Pyr]Ac- Ni0 |
11.3 |
|
nm |
XRD |
The average crystallite size was determined for the most intense peak at 2θ = 44.5° using the Debye Scherer equation was found to be 11.3 nm. |
|
|
|
|
|
|
|
|
8031 |
832 |
Au SRNPs |
140 |
|
nm |
SEM |
Figure S1 in the Supporting Information shows the scanning electron microscopy (SEM) images of SRNPs and QSNPs with nominally the same particle diameters of ∼140 nm. |
|
|
|
|
|
|
|
|
8076 |
881 |
FePOs |
420~430 |
|
nm |
DLS |
FePOs measured by DLS was approximately 420∼430 nm |
|
|
|
|
|
|
|
|
8077 |
882 |
Magnetite |
19(4) |
|
nm |
TEM |
the TEM micrographs of the nanoparticles electrochemically synthesized as well as the size distribution in the inset; thereof, the mean value is approximately 19(4) nm. |
|
|
|
|
|
|
|
|
8078 |
883 |
PVP-PtNC |
45.3 ± 14.0 |
|
nm |
|
|
|
|
|
|
|
|
|
|
8084 |
889 |
Ptn-JP NCs |
1.09-1.96 |
|
nm |
TEM |
Here, the size of Pt NCs inside Ptn-JP NCs was measured by TEM. As shown in Fig. 1 and Fig. S2,† Pt NCs inside Ptn-JP NCs exist in a good monodisperse state. The calculated average diameters of Pt NCs inside Pt50-JP, Pt200-JP and Pt400-JP were 1.09 ± 0.23 nm, 1.78 ± 0.53 nm and 1.96 ± 0.59 nm, respectively. |
|
|
|
|
|
|
|
|
8087 |
895 |
BSA-MgNPs |
6 |
|
nm |
TEM |
The particle size distribution pattern (Figure 1A, inset) revealed that the major population of particles is in the range of 4−8 nm size with an average size distribution of 6.0 nm. |
6.53 m2 g−1 |
|
|
|
|
|
|
|
8088 |
896 |
Ptn-PEI NPs |
3.21-3.70 |
|
nm |
TEM |
Figure 3. TEM images and relevant size distribution of Pt NPs inside of (a) Pt50-PEI, (b) Pt100-PEI, and (c) Pt150-PEI. Pt NPs stabilized by PEI had a small size from 3.21 to 3.70 nm. |
|
|
|
|
|
|
|
|
8095 |
903 |
AuNPs |
10 |
|
nm |
SEM |
Figure 6. The SEM and energy spectral pictures |
|
|
|
|
|
|
|
|
8100 |
908 |
Au(111) |
|
|
|
|
|
|
|
|
|
|
|
|
|
8120 |
1057 |
Au NBPs |
|
|
|
|
Finally, after purification, two new absorption peaks at about 684 nm and 510 nm were the longitudinal and transverse LSPR peaks of Au NBPs, respectively. |
|
|
|
|
|
|
|
|
8119 |
1057 |
Cu2O@Ab2 |
245 |
|
nm |
SEM |
Meanwhile, in Fig. 1c, the particle size analysis further proved that Cu2O octahedrons presented a sharper size distribution of 245 nm in average. |
|
|
|
|
|
|
|
|
8144 |
1078 |
Au NPs |
17 |
|
nm |
TEM |
|
|
|
|
|
|
|
|
|
8145 |
1079 |
Copper Nanozyme |
15-20 |
|
μm |
SEM |
|
|
|
|
|
|
|
|
|
8162 |
1098 |
Au NCs |
8 |
|
nm |
TEM |
文章没说 自己量的 |
|
|
|
|
|
|
|
|
8175 |
1110 |
AgPd0.38 |
|
|
|
TEM |
60–75 nm under TEM, 125–145 nm in water |
|
|
|
|
|
|
|
|
8180 |
1118 |
Cu NanoZyme |
100 |
|
nm |
SEM |
The deposited nanoparticles on the surface of the fabric showed the presence of sub-100-nm quasi-spherical copper nanostructures as observed in the SEM image |
|
|
|
|
|
|
|
|
8187 |
1127 |
1-Me-D-Trp@AuNCs |
2.3 |
|
nm |
TEM |
The average diameter of the 1-Me-D-Trp@AuNCs estimated with TEM was about 2.3 nm (ESM Fig. S3). After the addition of NOR, the diameter of 1-Me-D-Trp@AuNCs-NOR increased to 5.2 nm (Fig. 4), indicating NOR adsorption onto the surface of the nanozymes. |
|
|
|
|
|
|
|
|
8199 |
1148 |
Pd NCs |
1.7 |
|
nm |
TEM |
According to TEM images, Pd NCs exhibits the average diameter of 1.7 nm (Fig. 1c). |
|
|
|
|
|
|
|
|
8210 |
1165 |
CuNFs |
400-500 |
|
nm |
SEM |
The SEM image in Fig. 1h shows the flower-like structures of CuNFs with an average size of 400–500 nm, having hierarchical structures with high surface-to-volume ratios. |
|
|
|
|
|
|
|
|
8240 |
1209 |
Cu/CeS |
|
|
|
|
|
|
|
|
|
|
|
|
|
8298 |
1287 |
GNE-based Au NPs |
27.5 |
|
nm |
TEM |
Average |
|
|
|
|
|
|
|
|
8302 |
1296 |
Ag |
45 |
|
nm |
DLS |
Average |
|
|
|
|
|
|
|
|
8303 |
1296 |
Au |
55 |
|
nm |
DLS |
Average |
|
|
|
|
|
|
|
|
8304 |
1297 |
Rh NPs |
40.9 |
18.2 |
nm |
TEM |
hydrodynamic diameters |
|
|
|
|
|
|
|
|
8310 |
1298 |
Au*NPs |
4.1 |
0.6 |
nm |
DLS |
hydrodynamic diameters |
|
|
|
|
|
|
|
|
8309 |
1298 |
Pt*NPs |
5.4 |
0.8 |
nm |
DLS |
hydrodynamic diameters |
|
|
|
μmol/min |
|
|
U/mg |
|
8308 |
1298 |
Pt NPs |
8.6 |
1.4 |
nm |
DLS |
hydrodynamic diameters |
|
|
|
|
|
|
|
|
8307 |
1298 |
RhNPs |
7.8 |
1.2 |
nm |
DLS |
hydrodynamic diameters |
|
|
|
|
|
|
|
|
8305 |
1298 |
AuNPs |
6.6 |
0.9 |
nm |
DLS |
hydrodynamic diameters |
|
|
|
μmol/min |
|
|
U/mg |
|
8306 |
1298 |
RuNPs |
6.6 |
0.9 |
nm |
DLS |
hydrodynamic diameters |
|
|
|
|
|
|
|
|
8311 |
1298 |
PdNPS |
36.8 |
4.8 |
nm |
DLS |
hydrodynamic diameters |
|
|
|
|
|
|
|
|
8328 |
1317 |
Pd |
|
|
|
TEM |
|
|
|
|
|
|
|
|
|
8330 |
1323 |
PtDEN |
40 |
|
nm |
SEM |
|
|
|
|
|
|
|
|
|
8334 |
1326 |
SBA-AmPA/Au |
600-700 |
|
nm |
SEM |
|
|
|
|
|
|
|
|
|
8348 |
1344 |
AgNCs |
2.8 |
|
nm |
TEM |
TEM images displayed an average size of AgNCs of 2.80 nm. |
|
|
|
|
|
|
|
|
8360 |
1354 |
Au NPs |
20 |
|
nm |
TEM |
The size and shape of the Au NPs formed with 50 mU mL–1 concentrated ACP were ∼20 nm and spherical, respectively. |
|
|
|
|
|
|
|
|
8407 |
1397 |
citrate-Os NPs |
1.7 |
|
nm |
TEM |
The average diameter of the citrate-Os NPs obtained from the TEM images was 1.7 nm adjusted by Gaussian tting |
|
|
|
|
393 |
|
U/mg |
|
8424 |
1417 |
Au@SiO2@Fe3O4@SiO2 microspheres |
5.3 |
|
μm |
|
|
|
|
|
|
|
|
|
Median pore
size is 23.4 nm |
8440 |
1435 |
PdNCs |
57 |
|
nm |
TEM |
The average |
|
|
|
|
|
|
|
|
8441 |
1436 |
Ag@PANI |
50 |
|
nm |
SEM |
The average |
|
|
|
|
|
|
|
|
8451 |
1450 |
2D SnSe |
|
|
|
AFM |
To assess the impacts of SnSe morphologies, we compared the catalytic activities of SnSe spheres (10 nm) and nanosheets with different laminar layers (1.5 nm, 30 nm, 80 nm, 185 nm). |
|
|
|
|
|
|
|
|